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A flow-through reaction cell for studying minerals leaching by in-situ synchrotron powder x-ray diffraction
Journal article   Open access   Peer reviewed

A flow-through reaction cell for studying minerals leaching by in-situ synchrotron powder x-ray diffraction

F. Nikkhou, F. Xia, X. Yao, I.A. Adegoke, Q. Gu and J.A. Kimpton
Minerals, Vol.10(11), Article 990
2020
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Abstract

A flow-through reaction cell has been developed for studying minerals leaching by in-situ time-resolved powder X-ray diffraction, allowing for a better understanding of the leaching mechanisms and kinetics. The cell has the capability of independent control of temperature (up to 95 °C) and flow rate (>0.5 mL min−1) for atmospheric pressure leaching. It was successfully tested at the powder diffraction beamline at the Australian Synchrotron. Galena powder was leached in a citrate solution under flow-through condition at a flow rate of 0.5 mL min−1, while diffraction patterns were collected during the entire leaching process, showing rapid galena dissolution without the formation of secondary mineral phases. The flow-through cell can be used to study leaching processes of other ore minerals.

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Collaboration types
Domestic collaboration
Citation topics
7 Engineering & Materials Science
7.229 Mineral & Metal Processing
7.229.774 Bioleaching
Web Of Science research areas
Geochemistry & Geophysics
Mineralogy
Mining & Mineral Processing
ESI research areas
Geosciences
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