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Conversion of wood pyrolysates to PCDD/F
Journal article   Peer reviewed

Conversion of wood pyrolysates to PCDD/F

N.W. Tame, B.Z. Dlugogorski and E.M. Kennedy
Proceedings of the Combustion Institute, Vol.32(1), pp.665-671
2009
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Abstract

This contribution assesses the propensity of wood components to form polychlorinated dibenzo-p-dioxins and polychlorinated dibenzofurans (PCDD/F) in fires and in combustion in stoves, heaters and burn barrels. Volatiles generated from model lignocellulosic compounds or fractions isolated from wood are reacted with a surrogate ash positioned in a tubular reactor under inert pyrolysis atmospheres. The surrogate ash contains copper and chlorine salts to simulate heterogeneous PCDD/F formation during combustion of preservative-treated wood. Pyrolysis temperatures were selected to fall within the range in which the component decomposes, while the surrogate ash temperature was set at 400°C which is typical of pyrolysis during fires, and corresponds to conditions which were favourable to PCDD/F formation. PCDF are favoured over PCDD in all experiments. Lignin yields considerably more PCDD/F than the carbohydrates. The ratio of PCDD to PCDF varies according to the chemical structure of the feed; with carbohydrates demonstrating greater relative preference for PCDD than lignin. PCDD/F formation via direct chlorination of dibenzofuran and dibenzo-p-dioxin dominates the pyrolysis of lignin, as evidenced by a significant preference for 2,3,7,8 congeners. Carbohydrates likely produce PCDD/F as a result of formation and condensation of chlorophenol.

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Citation topics
3 Agriculture, Environment & Ecology
3.60 Herbicides, Pesticides & Ground Poisoning
3.60.221 Persistent Organic Pollutants
Web Of Science research areas
Energy & Fuels
Engineering, Chemical
Engineering, Mechanical
Thermodynamics
ESI research areas
Engineering
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