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Iminopropadienones R–NCCCO and carbon suboxide, C3O2. Theoretical and experimental 13C NMR spectra
Journal article   Peer reviewed

Iminopropadienones R–NCCCO and carbon suboxide, C3O2. Theoretical and experimental 13C NMR spectra

R. Koch, T. Bruhn, R.N. Veedu and C. Wentrup
Journal of Molecular Structure: THEOCHEM, Vol.686(1-3), pp.31-36
2004
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Abstract

The 13C NMR data of five iminopropadienones R–N6-point double bond; length half of m-dashC6-point double bond; length half of m-dashC6-point double bond; length half of m-dashC6-point double bond; length half of m-dashO as well as carbon suboxide, C3O2, have been examined theoretically and experimentally. The best theoretical results were obtained using the GIAO/B3LYP/6-31+G**//MP2/6-31G* level of theory, which reproduces the chemical shifts of the iminopropadienone substituents extremely well while underestimating those of the cumulenic carbons by 5–10 ppm. The computationally faster GIAO/HF/6-31+G**//B3LYP/6-31G* level is also adequate.

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Domestic collaboration
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Citation topics
2 Chemistry
2.1 Synthesis
2.1.834 Cycloaddition Reactions
Web Of Science research areas
Chemistry, Physical
ESI research areas
Chemistry
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