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The effects of halides in the electrowinning of zinc. I. Oxidation of chloride on lead-silver anodes
Journal article   Open access   Peer reviewed

The effects of halides in the electrowinning of zinc. I. Oxidation of chloride on lead-silver anodes

M. Nicol, C. Akilan, V. Tjandrawan and J.A. Gonzalez
Hydrometallurgy, Vol.173, pp.125-133
2017
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Abstract

A study of the kinetics of the anodic oxidation of chloride ions on the surface of lead-silver anodes used for the electrowinning of zinc has shown some interesting and practically important results. Oxidation of chloride does not occur on a PbSO4 surface but occurs readily on a PbO2 surface. Oxidation of chloride occurs at the mass-transport controlled rate at the operating potentials of anodes during the electrowinning of zinc in the absence of manganese in the electrolyte. However, the rate of oxidation of chloride ions is significantly lower in the presence of manganese ions in the concentration range 1 to 5 g/L. These results have been compared with plant observations that confirm the lower rate of chlorine generation in the presence of manganese. The use of periodic current reversal does not increase the rate of oxidation of chloride ions in the presence of manganese ions. The rate of anodic oxidation of chloride in the presence of manganese ions is too low to be of practical value in controlling the chloride levels during the electrowinning of zinc.

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Collaboration types
International collaboration
Citation topics
2 Chemistry
2.210 Corrosion & Deposition Chemistry
2.210.2222 Lead-Acid Battery
Web Of Science research areas
Metallurgy & Metallurgical Engineering
ESI research areas
Materials Science
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